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Go to Editorial ManagerThe objective of this paper is to develop an efficient P-wave detection algorithm based on the morphology characteristics of arrhythmias using time domain analysis.ECG from normal subjects, and patients with atrial fibrillation were studied. After baseline wander cancellation, power line interference filtration, the step of QRS detection using the pan- Tompkins algorithm is utilized to calculate R peak which represent the reference point to detect P peak.The algorithm was tested with experiments using MIT-BIH arrhythmia database which included Paroxysmal Atrial Fibrillation PAF prediction challenge, Massachusetts Institute of Technology MIT-BIH normal sinus rhythm, long term Atrial Fibrillation AF and MIT-BIH atrial fibrillation where every P-wave was extracted.The results reveal that the algorithm is accurate and efficient to detect and classify arrhythmias resulted from atrial fibrillation.
The Mono and binary-mixed oxide catalysts were prepared by precipitation and co-precipitation method and investigated for the photocatalytic decolorization of orange G dye which was used as a pollutant model in this study. The structure of the synthesized catalysts were characterized by the X-ray diffraction (XRD), bonding by fourier transfer infrared (FTIR), morphology by scanning electron microscope (SEM) and reflection using UV-VIS diffuse reflectance spectra. The XRD results revealed that the mono oxide catalysts confirm well the cubic phase of cadmium and cerium oxide and that their mixed oxide catalyst i.e. 50Ce/25Cd show the same characteristic peaks of pure cerium oxide with slight shift to higher wave lengths for two crystalline peaks at 33.15° and 56.15° respectively. The FTIR spectra of 50Ce/25Cd mixed oxide catalyst improved the combination between both pure cadmium and cerium oxide catalyst. The diffuse reflectance showed a blue shift towards lower wave length and that the energy gap was increased with an increase in cerium content. Different reaction variables such as, effect of metal content, pH values, amount of hydrogen peroxide and effect of catalyst amount were studied to estimate their effect on the decolorization efficiency of orange G dye. The maximum catalytic activity achieved was 91% at a solution pH of 2.1, catalyst dosage of 1.5 g/L, 0.15 mL of H2O2 /100 mL of reaction volume and initial dye concentration of 10 mg/L after 60 min of reaction time.
The Electrodeposition process has been used to prepare Nickel-Tungsten alloys on low carbon steel substrate by using ammonical citrate bath. The influence of deposition condition by variation of current density (0.04-0.2 A/cm2) and solution temperature (60-70 °C), on the microstructure was studied. The optical microscope and the scanning electron microscopy (SEM) were used to study the morphology of the deposit while the energy dispersive spectroscopy (EDS) was used to approximate the composition, in addition to X-Ray diffraction examination. The results show that the current efficiency has the major influence on the tungsten content in the alloys due to the formation of ternary complex which reflected into the properties of the deposit._x000D_ Keywords:
The aim of this work is to optimize EPD variables (voltage, time, and focus) using alternating current through the Taguchi Design of Experiment (DOE). Coating Nano hydroxyapatite (Nano-HA) on a Ti6Al4V substrate depends on thickness and roughness, then characterization of a coating layer to determine the optimum state. Hydroxyapatite (HAp) powder was deposited on a Ti-6Al-4V alloy substrate by electro-deposition with ethanol as a solvent under AC current, to improve the alloy surface quality based on coating thickness and maximum coating mass meeting the requirements of a biological orthopedics application. Ethanol was used as a solvent to precipitate ketazone and HAp on the base alloy. Taguchi's approach was used in order to determine the optimal conditions for EPD and subsequently to apply various criteria for depositing the biochemical coating. The surface and cross-section composition of the paint is described by characterization. Numerous tests and inspections; Zeta, XRD and SEM stability test, water contact angle and optical microscopes were used to describe the surface morphology of the HAp layer. The value of the optimum conditions for deposition of the HAp layer which is a simultaneous thickness and maximum coating mass, was predicted at a sedimentation voltage of 40 V, 2 min sedimentation time and 1 g / L for the concentration of the suspended solution at room temperature. The validity of the model resulting from the response surface methodology was assessed by comparing the expected results with the experimental results. In addition, close agreement was observed between the experimental results and the expected results. For the solution at room temperature, the results obtained with the highest value of the coating thickness of 41at the surface roughness of 0.94 and the contact angle of the alloy before coating is 67.489º reduced to. 38.132º after plating, which indicates an increase in the harmony of the metal implant and biocompatibility.
The present work was designed on producing nanohydroxyapatite layers using electrophoretic deposition (EPD) on 316L stainless steel substrate. The EPD coatings were prepared by the deposition of hydroxyapatite (HA)-chitosan nanocomposites on different substrate roughness (polish surface, 220 grit SiC grind, and sand blast surfaces). Depositions were performed using the suspensions of HA nano particles (3 g/L) in the mixture of alcohol and distilled water (ethanol, 5 vol. %water and containing 0.5 g/L of chitosan dissolved in 1 vol.% acetic acid. Coatings were achieved on the cathode at constant voltage, time and temperature (90 V, 5 min and 40 °C respectively); the pH value was performed and fitted at 4. After deposition, the coated samples were dried at room temperature for 24 h. The surface topography of coatings was analyzed using atomic force microscopy (AFM). SEM was used to postulate both the surface and the cross section morphology of the coatings. The adhesion bonding between the deposited coatings and substrate were measured using tape tester to evaluate the adhesion bonding between the coating and substrate. The results showed the deposited coatings on sand blasted substrate has less porosity compared with the polish surface and 220 emery paper SiC grinding substrate respectively. The coating on the sand blasted substrate showed higher nanoroughness (122 nm), better adhesion bonding (removal area 15%) and higher thickness layer (12 µm) than that of the polish substrate and 220 emery paper SiC grinding substrate.
Surface reconstruction of silicon using lasers could be utilized to produce silicon nanostructures of various features. Electrochemical and photoelectrochemical etching processes of silicon were employed to synthesize nanostructured surface. Effects of current densities 5, 10 and 20 mA/cm2 on the surface features were examined. It is found that the surface porosity and layer thickness increase with the current density. Moreover, large surface area of 410 m2/cm3 can be achieved when laser power density 0f 0.6 W/cm2 was used during the etching process. Optimum operating conditions were found to achieve better silicon nanostructured surface features. The surface roughness can be reduced to 8.3 nm using laser beam of 650 nm irradiated the silicon surface during the photoelectrochemical etching process. The surface morphology of the nanostructured silicon surface using SEM and AFM could give rich details about the surface. Silver nanoparticles of 10 – 20 nm was embedded at the nanostructured silicon surface by LIFT process to reduce the surface resistance and maintain the large surface area. This technique enables silicon nanostructures to be efficiently used in many optoelectronic applications.
In this research, we successfully obtained Ni/SiC micro-composite coatings with various contents of SiC particles of particle size(10 ?m), by using electrodeposition method from nickel watts bath in which the SiC particles suspend. The effects of the current density, temperature, and particle loading(PL) of SiC particles in the electrolyte on the morphology, texture, and vol% of SiC in deposit were investigated. The morphological and structural analysis show uniform distribution of SiC particles within the composite coatings. It was found that the depositing conditions affect the microstructure of deposited nickel and the SiC vol% in deposit. Furthermore, the vol% of SiC increases in deposit by increasing the particle loading(PL) in the bath, while decreased by increasing the current density. Also the higher values of SiC vol% were obtained at temperature (50°C).
Poly(vinyl chloride) photodecomposition films that contains melamine Schiff base (0.5% by weight) as photostabilizers upon preservation with an ultraviolet light (UV) was investigated. The photodecomposition rate constant was reduced significantly in existence of melamine Schiff base compared to PVC (blank). The Schiff base 1 was found to most effective additive in PVC photostabilization films. Photodecomposition rate content for PVC films containing Schiff base 1 was found to be 5 × 10-3 sec-1 compared to 8.7 × 10-3 sec-1 for blank film. Ultraviolet radiation aging behaviors of PVC films were studied through leaching test by measuring the degree of migration. The surface morphology of PVC films was inspected by scanning electron microscope.
Optical coherence tomography (OCT) allows for direct and immediate imaging of the morphology of retinal tissue. It has become a crucial imaging modality for diagnosing eye problems in ophthalmology. One of the most significant morphological characteristics of the retina is the structure of the retinal layers, which provides important evidence for diagnostic purposes and is related to a variety of retinal diseases. In this paper, a convolutional neural network (CNN) model is proposed that can identify the difference between a normal retina and three common macular diseases: Diabetic macular edema (DME), Drusen, and Choroidal neovascularization (CNV). This proposed model was trained and tested on an open source dataset of OCT images also with professional disease classifications such as DME, CNV, Drusen, and Normal. The suggested model has achieved 98.3% overall classification accuracy, with only 7 wrong classifications out of 368 test samples. The suggested model significantly outperforms other models that made use of the identical dataset. The final results show that the suggested model is particularly adapted to the detection of retinal disorders in ophthalmology centers.
The efficiency of adsorption using copper nanocomposite catalysts for the removal of lead ions from aqueous solution was studied. Nano copper and its nanocomposition were prepared in laboratory in very accurate conditions. After preparing samples, the samples were analyzed using XRD and SEM and that shows very good morphology of catalytic performance and has nano sized of crystalline shape. In order to study the efficiency of these catalysts, all samples were tested using adsorption process. The preparing samples show very good efficiency for lead removing from aqueous solution, and reach maximum removal efficiency 96% for 0.05g of adsorbents at pH 10, otherwise increasing or decreasing the pH would give undesirable results for all samples. Langmuir isotherm fitted better than Freundlich isotherm for adsorption of lead.
This research investigates the influence of single and hybrid mineral nanofillers on the morphological, thermal, and electrical properties of epoxy-based glass fiber composites. Nanocomposites were fabricated using hand lay-up technique, incorporating nano-calcium carbonate (CaCO₃) and nano-talc with particle size of 50 to 100 nm into an epoxy matrix with 5-ply E-glass/S-glass fiber. The study evaluates composites with 2-8 wt% of nano-CaCO₃, and hybrid systems containing nano-CaCO₃ (2-8 wt%) and nano-talc (1-4 wt%). Morphological analysis via Scanning Electron Microscopy (SEM) assessed nanofiller dispersion, while thermal properties were analyzed using Differential Scanning Calorimetry (DSC) for glass transition temperature (Tg). Electrical performance was evaluated through dielectric breakdown voltage (ASTM D149) and surface resistivity (ASTM D257). SEM analysis showed filler dispersion depended on concentration, with optimal distribution at 4-6 wt% before significant agglomeration at higher concentrations. DSC results revealed increased Tg with nanofillers, peaking for the composite with 6 wt% CaCO₃ and 3 wt% talc, indicating enhanced thermal stability. The dielectric breakdown voltage peaked at 17.6 kV for 2 wt% CaCO₃ and 1 wt% talc composite, while surface resistivity was highest for 4 wt% CaCO₃ and 2 wt% talc (73.74×1012Ω). All formulations maintained UL 94 V-1 flammability rating. The study concludes that the synergistic interaction between nano-CaCO₃ and nano-talc enables significant tailoring of thermal and electrical properties for advanced applications.
Electrospinning is a simple and highly versatile method for generating ultrathin fibers (mainly polymers) with diameters ranging from a few micrometres to tens of nanometres. This technique has attracted tremendous recent interest in both academia and industry, owing to its unique ability to produce ultrafine fibers of different materials in various fibrous assemblies. Electrospinning is a process that uses an electric potential to overcome the surface tension of a solution to produce an ultra-fine jet, which elongates, thins and solidifies as it travels through the electric field to a collector.. In this research, we studied the effect of conditions of the cabin “specifically humidity” on the diameter of nanofibers manufactured by electrospinning. We used Polyvinyl alcohol (PVA) polymeric solution with weight concentration of 10%, voltage 20 kv, under different values of relative humidity. Fiber morphology and fiber diameter were determined using scanning electron microscope, and measuring the fiber diameter by using image j program. It was found that the diameter of the fibers increased with increasing the relative humidity within our studying area .
This paper presents a comparison of using different techniques for stir spot welding of Aluminum 2024-T3, which are refill friction stir spot welding (RFSSW), edited (RFSSW-pin) and conventional friction stir spot welding (FSSW), depending on the obtained tensile shear strength property. Specimens were prepared from AA2024-T3 sheet for chemical analysis and mechanical tests. Workpieces were stir spot welded utilizing the above mentioned techniques at four rotational speeds (2000, 2500, 3000 and 4000 rpm) using tool pin diameters (5 and 7 mm) for conducting the tensile shear tests. The microhardness along the cross section of the welded specimens was conducted at the best conditions as well as the microstructure examination. The comparison results revealed that at the rotational speeds (2000 and 4000 rpm) in both cases of tool pin (5 and 7 mm), the ultimate tensile shear force was slightly higher than that for other speeds. However, the ultimate tensile shear force was found higher at 3000 rpm speed with a tool pin 7 mm. The microhardness results manifested a W-shape at the best conditions. Finally, the microstructure examination depicted the morphology of the main zones of the weld joint.