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Search Results for raman

Article
Preparation and Characterization of Multilayer Graphene via Electrochemical Exfoliation in NaCl Solution

Aseel Hamza

Pages: 466-472

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Abstract

Graphene is two Dimension-carbon based nanomaterial, and unique properties of the graphene made it interest to researchers. The objective of this work was to address the need for low-cost, efficient graphene preparation; the electrochemical exfoliation process and photosynthesis of the exfoliated solution were used. In this study, the exfoliated graphite mixture. The exfoliated graphite (Gr2, Gr3, Gr4) (0.08, 0.1, 0.2 M NaCl, respectively) was dried by sunlight and investigated; the results confirmed of multilayer graphene by Raman, UV–Vis, FESEM/EDS, grain size 4–9 µm) . Behavior of UV analysis related with number of single and multilayer of graphene depends on conjugative effect that arises from nanometer-scale sp2 clusters, and chromophore units as well as functional groups, also oxygen clusters may be removed and disappear the shoulder. FTIR peaks confirmed peeling off graphene layers. One of the most important reactions is the incorporation of Cl atoms into unsaturated sites.  Grain size increased with increasing voltage, while it decreased in (0.2 M) NaCl.  FESEM showed a smooth, crimped surface. EDS analysis showed a C/O ratio of (7.6, 4.6, 1.26), with Cl and Na observed in rinsed Gr3. D, G, and 2D peaks were displayed by Raman spectroscopy. In this study, it was concluded that NaCl-assisted exfoliation is a simple and low-cost route.

Article
Performance Investigation of DP-16QAM Ultra-wideband- Wavelength-Division Multiplexing Communication System: Optimum Power Consideration

Arwa Moosa, Raad Sami Fyath

Pages: 37-44

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Abstract

Recently, there is increasing interest in using the 18 THz bandwidth offered by S+C+L band to increase the transmission capacity of fiber communication systems. This leads to the generation of ultra-wideband (UWB) wavelength-division multiplexing (WDM) optical communication systems. In these advanced systems, stimulated Raman scattering (SRS) causes a power transfer from high-frequency channels to low-frequency channels. This effect leads to an increase in the nonlinear interference (NLI) between the UWB-WDM channels. Power optimization techniques are required to balance transfer power between band channels, thus increasing the maximum transmission reach (MTR) along with increasing system capacity. In this paper, the transmission performance of S+C+L band system operating with dual-polarization 16-QAM signaling is investigated using enhanced Gaussian noise model. The transmitter and receiver for each DP channel use a -polarized laser and incorporate two identical configurations, one for x- and the other for y-state of polarization (SOP). The results are presented for two values of symbol rate, 40 and 80 GBaud, where the system carries 360 (=160+80+120) and 180 (=80+40+60) channels, respectively. The results revel that the MTR of both cases is equal to 12 100 km-spans when the channel lunch power equals to -4 and -2 dBm, respectively. This work also shows the effect of NLI components as a function of the number of spans, channel spacing, and channel launch power. The results show that the cross-phase modulation component of the NLI has high accumulated value with transmission distance, while the self-phase modulation component is almost constant.

Article
Toward Seven-Band Coherent WDM System Covering T to U Bands: Predictions of Transmission and BER Performance

Arwa A. Moosa, Raad Sami Fyath

Pages: 61-77

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Abstract

This paper discusses the development of a seven-band coherent wavelength-division multiplexing (WDM) system covering the T to U systems, aiming to enhance the capacity and system efficiency. Seven multiband systems (C+L, S+C+L, S+C+L+U, E+S+C+L, E+S+C+L+U, O+E+S+C+L+U, and T+O+E+S+C+L+U) are designed with 40 GBaud symbol rate, 50 GHz channel spacing, and dual-polarization (DP)-16QAM signaling. The analysis adopted the enhanced Gaussian noise model, considering the amplified spontaneous emission of inline optical amplifiers and nonlinear interference (NLI) from fiber nonlinear optics, including Kerr effect and stimulated Raman scattering (SRS) which it implemented using Matlab (Ver. 2020b) program. The results show that the optimal powers are -4, -5, -5, -4.5, -3.5, -6, and -4.5 dBm for the seven WDM systems, respectively. Further, with a fiber span length of 100 km, the C+L system has the longest transmission reach of 20 span. However, using S+C+L+U system gives the highest bit rate-distance product of 1619 Tbps.km. The O+E+S+C+L+U and T+O+E+S+C+L+U systems are designed with 50 km-span length to reduce the effect of NLI caused by the large numbers of channels (1060 and 1200, respectively).

Article
Laser Produced Hydrophilic and Hydrophobic Silicon Surfaces

A. A. Hatem, B. G. Rasheed, Naser M. Ahmed

Pages: 54-60

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Abstract

Two lasers were utilized for silicon processing using photoelectrochemical etching and laser texturing in order to produce nano/micro structures, respectively. Photoelectrochemical etching process utilizes a CW diode laser of 532 nm wavelength was used to support electrochemical etching for both n-type and p-type conductivity. While laser texturing process was employed using pulsed fiber laser of 1064 nm wavelength. Various characterization methods were devoted to examine silicon micro/nanostructures surfaces produced by lasers. These methods include AFM, SEM and Raman scattering to provide clear evidence about formation of micro/nanostructures abundant at silicon surfaces.  Moreover, FTIR analysis for the laser produced silicon surfaces could emphasize whether the resultant silicon surface is hydrophilic or hydrophobic. Image analysis software adopted a side view micro image was used to measure the contact angle between the water droplet and silicon micro/nano-surfaces. It is found that the laser produced silicon nanostructure by photoelectrochemical etching creates a hydrophobic surface and even super hydrophobic with contact angle of 130 degrees for 50 nm average size. In addition, utilizing fiber laser of high repetition rate for laser texturing produces microstructures that are super hydrophilic with contact angle could reach 8 degrees for a surface dimension of 50 μm.

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