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Go to Editorial ManagerGraphene is two Dimension-carbon based nanomaterial, and unique properties of the graphene made it interest to researchers. The objective of this work was to address the need for low-cost, efficient graphene preparation; the electrochemical exfoliation process and photosynthesis of the exfoliated solution were used. In this study, the exfoliated graphite mixture. The exfoliated graphite (Gr2, Gr3, Gr4) (0.08, 0.1, 0.2 M NaCl, respectively) was dried by sunlight and investigated; the results confirmed of multilayer graphene by Raman, UV–Vis, FESEM/EDS, grain size 4–9 µm) . Behavior of UV analysis related with number of single and multilayer of graphene depends on conjugative effect that arises from nanometer-scale sp2 clusters, and chromophore units as well as functional groups, also oxygen clusters may be removed and disappear the shoulder. FTIR peaks confirmed peeling off graphene layers. One of the most important reactions is the incorporation of Cl atoms into unsaturated sites. Grain size increased with increasing voltage, while it decreased in (0.2 M) NaCl. FESEM showed a smooth, crimped surface. EDS analysis showed a C/O ratio of (7.6, 4.6, 1.26), with Cl and Na observed in rinsed Gr3. D, G, and 2D peaks were displayed by Raman spectroscopy. In this study, it was concluded that NaCl-assisted exfoliation is a simple and low-cost route.
The present work deals with direct diffusion bonding welding without interlayer of austenitic stainless steel type AISI 304L with Oxygen Free High Conductivity pure copper (OFHC) in vacuum atmosphere (1.5 *10-5 mbr.). The optimum bonding conditions are temperature of 650 ?C, duration time of 45 min. and the applied stress of 30 MPa, in order to secure a tight contact between the mating surfaces. The corrosion behavior of diffusion bonding joints in 3.5% Nacl is studied to evaluate the corrosion resistance of welding joints by using Potentiodynamic method. The observed microstructure of corroded specimen of optimum diffusion bonding joint shows that the corrosion current density has low value as compared with base materials used. During polarization, galvanic coupling is observed between two materials used. At passivity region, inverse polarity is occurred at 450mV. Therefore, passive stainless steel 304 L behaves as cathode respective to pure copper, the corrosion behavior of the diffusion bonding joint was mostly by copper side. The corrosion results indicate the presence of galvanic effect. The corrosion current density of copper, stainless steel 304L and bond joints condition were (3.66 µA/cm2, 1.62 µA/cm2 and 1.85µA/cm2) respectively. A SEM examination of corroded diffusion bonding joint indicates that the galvanic corrosion happened on copper side. The corrosion rate of bonding joint conditions was 0.85 mpy, which is less than 1%. This means that corrosion resistance of bond joint is more than excellent.
This research study the rheological properties ( plastic viscosity, yield point and apparent viscosity) of non-Newtonian fluids under the addition of different chemical additives with different concentrations, such as (xanthan gum (xc-polymer) , carboxy methyl cellulose ( high and low viscosity ) ,polyacrylamide, polyvinyl alcohol, starch, quebracho, chrome lignosulfonate, and sodium chloride (NaCl). Fann viscometer model 800 with 8-speeds was used to measure the rheological properties of these samples, that have already been prepared. All samples were subjected to Bingham plastic model. It was concluded that the plastic viscosity, yield point and apparent viscosity should be increased with increasing the concentrations of (xanthan gum (xc-polymer) , carboxy methyl cellulose ( high and low viscosity ) ,polyacrylamide, polyvinyl alcohol, starch and sodium chloride (NaCl), while the opposite is true for quebracho, chrome lignosulfonate.
Whispering Gallery Mode Micro-Resonators (WGMRs) have received significant interest due to their great sensitivity to environmental changes, compact size, and ability to operate over a wide spectral range because their low optical losses produce high-quality factors so that they can be used in various sensing applications. This work investigates the design and implementation of cylindrical WGMRs for Refractive Index (RI) sensing for different delivery fiber diameters. Single Mode Fiber with different waist diameters (80,67.1,18) µm were used as delivery fibers. At the same time, the sensor (resonator) fiber is SMF with a diameter (125 µm). Quality factors and Free Spectral Range (FSR) were calculated and analyzed for each diameter. The quality factor for all diameters was in power of 104, which is considered good. The FSR is inversely proportional to fiber diameter. FSR values were (0.678,1.75,2.03) nm for (80,67.1,18) µm delivery fiber diameters respectively. An analyte prepared by NaCl with different refractive indices is used to investigate the RI sensor performance. Higher sensitivity is obtained from the WGMR with a smaller waist diameter, which is (-)74 nm/RIU. While for the delivery fiber diameters (80,67.1) µm were (-0.28, -9.27) nm/RIU respectively. The submitted sensor will have a good contribution in the field of chemical, biological and medical applications.