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Go to Editorial ManagerHigh-performance polymer nanocomposites utilizing different-sized nanofillers had a lot of interest recently. Due to their distinct structural, and thermal characteristics. Multi-wall carbon nanotubes (MWCNT) and nanoclay (NC) have the most interest among the numerous types of reinforcing as filler elements for a polymer. The formation of hybrid from MWCNT and NC at various loadings (0.5%, 1%, and 2wt%) on the characteristics of epoxy polymer have been assessed in this work. The specimens have been created using solution blending procedures with the addition of solvent ethanol at a ratio of 1:1 for dispersed nanofillers, and then they have been re-mixed with epoxy. Tests like X-Ray diffraction (XRD), and thermal conductivity were used to identify properties of epoxy. According to the test results, the thermal conductivity rise as the filler content rises at 1wt%, then start to decrease after 1wt%. The sample with the hybrid filler loading of 1 wt% produced the best performance. Since hybrid epoxy exhibits the best result of the thermal conductivity 135% over MWNT and NC nanocomposites of 1 wt.% reached 0.3568 W/m.K in the increased thermal conductivity property. By examining the EP nanocomposites XRD pattern. The hybrid of epoxy nanocomposites exhibits all of the NC and MWCNT characteristic peaks. Since interactions between the filler and the epoxy cause a shift in the peak location of 1wt%. Due to the homogeneity of the nanofillers entire epoxy matrix, there may be changes in the intensity or location of the peaks at 1% for 2θ= 20.13°, which corresponds to an interlayer distance of d=0.461nm.
This research investigates the influence of single and hybrid mineral nanofillers on the morphological, thermal, and electrical properties of epoxy-based glass fiber composites. Nanocomposites were fabricated using hand lay-up technique, incorporating nano-calcium carbonate (CaCO₃) and nano-talc with particle size of 50 to 100 nm into an epoxy matrix with 5-ply E-glass/S-glass fiber. The study evaluates composites with 2-8 wt% of nano-CaCO₃, and hybrid systems containing nano-CaCO₃ (2-8 wt%) and nano-talc (1-4 wt%). Morphological analysis via Scanning Electron Microscopy (SEM) assessed nanofiller dispersion, while thermal properties were analyzed using Differential Scanning Calorimetry (DSC) for glass transition temperature (Tg). Electrical performance was evaluated through dielectric breakdown voltage (ASTM D149) and surface resistivity (ASTM D257). SEM analysis showed filler dispersion depended on concentration, with optimal distribution at 4-6 wt% before significant agglomeration at higher concentrations. DSC results revealed increased Tg with nanofillers, peaking for the composite with 6 wt% CaCO₃ and 3 wt% talc, indicating enhanced thermal stability. The dielectric breakdown voltage peaked at 17.6 kV for 2 wt% CaCO₃ and 1 wt% talc composite, while surface resistivity was highest for 4 wt% CaCO₃ and 2 wt% talc (73.74×1012Ω). All formulations maintained UL 94 V-1 flammability rating. The study concludes that the synergistic interaction between nano-CaCO₃ and nano-talc enables significant tailoring of thermal and electrical properties for advanced applications.
The mechanical behavior of multilayer FRCMs was tested, and the effects of fibers, types of fiber, and laminates on the tensile, flexural, and impact properties were discussed. The vacuum bagging method is a composite manufacturing process that uses atmospheric pressure to consolidate laminate layers, remove excess resin, and get rid of air bubbles. This makes high-quality, void-free composites. Four composite systems were made using this method: natural fiber composites reinforced with sheep wool and goat hair fibers, and synthetic fiber composites reinforced with carbon and glass fibers, all with an epoxy resin (LR620) and hardener (LH620) system. All composite assemblies have been systematically characterized at different layer configurations (3-6 layers considered) for the best structural response. The tensile, flexural, and impact properties were tested by following the corresponding ASTM (D638, D790, D6110) standards, respectively. The tensile and flexural results of the carbon fiber composite (GCT, GCB series) showed excellent mechanical performance (maximum tensile strength of 283 MPa for GCT4 and flexural strength of 164 MPa for GCB5) with high load-carrying capacity, but the failure was brittle. Goat hair composites exhibited excellent impact resistance (GHI4: 1.255 J) and moderate tensile strength (36 MPa), which indicated superior energy absorption capacity. The glass fiber composites showed a good balance of mechanical properties with increased ductility, where the tensile strength was 245 MPa, and a large deflection capacity was reached (14.683 mm). The study demonstrates that 4-layer setups usually result in the highest tensile properties, while 5–6-layer setups improve the flexural strength. These results add to the knowledge of optimization of multilayer composite design, and they are very useful for materials selection in aerospace, automotive, and structural applications.
Particles filled polymer composites started to be essential because of their wide applications in addition to reducing the cost of polymer, which is a main problem. The aim of this work is studying the insulation of particulate composites resulting from the addition of filler (glass or porcelain) waste powder to reinforced epoxy matrix. Samples with and without filler were exposed to some tests to decide the influence of the filler contents on the characteristics of epoxy. Epoxy is synthesized with filler particles having (90 micron) particle sizes as reinforcement. Composites of epoxy with varying percentage (0 to 40 weights %) of filler were prepared by using hand lay-up method. The nondestructive tests consist of thermal conductivity; ultrasonic test and water absorption test have been investigated. The composite showed an improvement in physical properties with the addition of filler according to their percentages. The result show the addition of the filler in all proportions to the epoxy increased the density of the composite, leading to the ultrasonic pulses velocity ranges between 2100 m/s and 2800 m/s. Increase glass and porcelain percentage cause increase in density which increases the acoustic impedance. While the thermal conductivity decrease with glass powder percentages in the composite increase, unlike the increase in porcelain percentage which causes an increase in thermal conductivity. The 40% percentage of glass in the epoxy had higher effect on reduce the thermal conductivity. As well as from the results the epoxy reinforced by porcelain powder would have lower water absorption than epoxy reinforced by glass powder.