Vol. 29 No. 2 (2026) Cover Image
Vol. 29 No. 2 (2026)

Published: June 20, 2026

Pages: 282-290

Articles

Effect of Date Seeds Ash Incorporation with Micro Silica on the Cement Mortar Behavior and Mix Integrity

Abstract

This study evaluates the performance of cement mortar incorporating micro silica (MS) and thermally treated date seed ash (DS) as sustainable partial cement replacements, in line with the demand for improved construction materials that utilize available resources. In the absence of an understanding of the behavior resulting from combining MS and DS within a hybrid replacement system particularly regarding how different blending ratios influence mortar performance and mix integrity. To achieve this,  five mixtures were prepared with a total replacement level of 20%  including three hybrid blends and were assessed through flowability, compressive strength, sorptivity, dry density, water absorption, and Ultrasonic Pulse Velocity (UPV) tests. Predictive models  have  also been developed to estimate chloride and sulfate penetration based on physical and non-destructive indicators. The results showed that the hybrid mixture  MS15–DS5  demonstrated the most notable enhancement compared to the control mix, achieving a 6% increase in compressive strength a 42% reduction in sorptivity and clear increases in dry density and pulse velocity indicating a more compact internal structure. The MS10–DS10 mixture also exhibited improved behavior, though to a lesser degree. In contrast, increasing the DS content led to performance deterioration, where MS5–DS15 showed reduced strength and higher sorptivity and DS20 presented the weakest response, with an 8% reduction in compressive strength and a 32% increase in sorptivity. The predictive models also demonstrated high accuracy achieving R2 of 0.989 and 0.983 for chloride and sulfate penetration, respectively, supporting their ability to estimate future behavior based on physical properties. These results provide a clearer understanding of how combining MS and DS influences mortar behavior and mix integrity, and they contribute to the development of sustainable cementitious mixtures with improved performance when appropriate replacement levels are selected.

References

  1. Y. Habibi, W. K. El‑Zawawy, M. M. Ibrahim, and A. Dufresne, "Processing and characterization of reinforced polyethylene composites made with lignocellulosic fibers from Egyptian agro‑industrial residues," Compos. Sci. Technol., vol. 68, no. 7-8, pp. 1877-1885, 2008. https://doi.org/10.1016/j.compscitech.2008.01.008
  2. M. Almograbi, "Durability study of lightweight concrete material made from date palm seeds (DPS)," WIT Trans. Built Environ., vol. 112, pp. 69-75, 2010. https://doi.org/10.2495/HPSM100071
  3. A. Adefemi, M. H. Nensok, E. T. Ka'ase, and I. A. Wuna, "Exploratory study of date seed as coarse aggregate in concrete production," Civil Environ. Res., vol. 3, no. 1, pp. 85-92, 2013.
  4. S. M. Akib, D. Bhuva, and D. Pindoriya, "Exploratory study on partial replacement of coarse aggregate by date seed," Int. Res. J. Eng. Technol., vol. 7, no. 4, pp. 730-734, 2018.
  5. A. Ahmed, S. A. Mangi, A. W. Muhammad, and N. U. Din, "Strength performance of concrete containing date seeds as partial replacement of coarse aggregates under the exposure of NaCl and Na₂SO₄," Indones. J. Soc. Environ. Issues, vol. 1, no. 3, pp. 205-211, Dec. 2020. https://doi.org/10.47540/ijsei.v1i3.104
  6. A. R. Palh, S. A. Mangi, M. A. Odho, and A. A. Kalhoro, "Experimental study on concrete incorporating date seed as partial replacement of coarse aggregates," Neutron, vol. 20, no. 2, pp. 113-122, 2021. https://doi.org/10.29138/neutron.v21i1.85
  7. S. J. Shah, S. Nath, A. Naeem, and E. Kakar, "Study on concrete mix with partial and full replacement of coarse aggregates with date seeds," J. Appl. Emerg. Sci., vol. 12, no. 2, pp. 219-224, 2022.
  8. S. C. Sarathkumar, C. Karthik, A. Anitha, and S. Suresh, "Experimental investigation on concrete with partial replacement of fine aggregate by date and tamarind seed," Int. J. Adv. Res. Ideas Innov. Technol., vol. 8, no. 1, pp. 45-52, 2022.
  9. R. Rajasekaran and T. Balamurugesan, "Experimental investigation on partial replacement of coarse aggregate by agro product waste in concrete," in AIP Conf. Proc., vol. 2861, art. 070003, Aug. 2023. https://doi.org/10.1063/5.0158370
  10. C. Elazizi, H. Hammi, W. Marzouk, H. Majdoub, and A. M'nif, "Effect of a partial replacement of Portland cement by date seeds on the mechanical and chemical behavior of the mortar," J. Tunis. Chem. Soc., vol. 19, pp. 326-334, 2017.
  11. G. I. Gunarani and S. P. Chakkravarthy, "Experimental studies on effect of date seed ash (DSA) on strength properties of cement sand mortar," IOP Conf. Ser.: Earth Environ. Sci., vol. 80, no. 1, p. 012015, Jul. 2017. https://doi.org/10.1088/1755-1315/80/1/012015
  12. Z. H. A. Alsalami, I. K. Harith, and M. K. Dhahir, "Utilization of dates palm kernel in high performance concrete," J. Build. Eng., vol. 20, pp. 166-172, 2018. https://doi.org/10.1016/j.jobe.2018.07.015
  13. A. S. J. Smith, "Investigation of date palm seed ash (DPSA) as pozzolana in concrete," M.S. thesis, Dept. Civ. Eng., Bayero Univ., Kano, Nigeria, 2018.
  14. M. K. Saeed, M. K. Rahman, M. Alfawzan, S. Basha, and H. A. Dahish, "Evaluation of date kernel powder (DKP) for potential use as setting and hydration retarder in concrete," J. Build. Eng., vol. 57, p. 104855, 2022. https://doi.org/10.1016/j.jobe.2022.104855
  15. M. K. Saeed, M. K. Rahman, M. Alfawzan, S. Basha, and H. A. Dahish, "Recycling of date kernel powder (DKP) in mass concrete for mitigating heat generation and risk of cracking at an early age," Constr. Build. Mater., vol. 376, p. 131033, 2023. https://doi.org/10.1016/j.conbuildmat.2023.131033
  16. M. K. Saeed, M. K. Rahman, M. Alfawzan, S. Basha, and H. A. Dahish, "Investigating the potential use of date kernel ash (DKA) as a partial cement replacement in concrete," Materials, vol. 15, no. 24, p. 8866, 2022. https://doi.org/10.3390/ma15248866
  17. S. K. Alkhaldi, "Reducing the carbon footprint and enhancing the strength of mortar (concrete) through the incorporation of date seeds ash," M.S. thesis, Alfaisal Univ., Riyadh, Saudi Arabia, 2023.
  18. I. B. Auta, I. I. Abdulkarim, and O. O. Olu, "Effect of date palm seed pod ash and eggshell powder on the physico‑mechanical properties of cement blends," Am. J. Sci. Eng. Technol., vol. 8, no. 1, pp. 1-12, 2023.
  19. B. H. Amanah and W. I. Khalil, "Effects of eggshells powder and date seeds on properties of sustainable concrete," AIP Conf. Proc., vol. 2864, no. 1, art. 060003, Jan. 2024. https://doi.org/10.1063/5.0186936
  20. ASTM International, ASTM C33/C33M‑08: Standard Specification for Concrete Aggregates, West Conshohocken, PA, USA, 2008.
  21. ASTM International, ASTM C150/C150M‑21: Standard Specification for Portland Cement, West Conshohocken, PA, USA, 2021.
  22. ASTM International, ASTM C1240‑20: Standard Specification for Silica Fume Used in Cementitious Mixtures, West Conshohocken, PA, USA, 2020.
  23. ASTM International, ASTM C1437‑15: Standard Test Method for Flow of Hydraulic Cement Mortar, West Conshohocken, PA, USA, 2015.
  24. L. G. Li, N. Pui‑Lam, Z. H. Huang, Z. J. Zhu, and A. K. H. Kwan, "Effects of micro‑silica and nano‑silica on fresh properties of mortar," Mater. Sci. (Medžiagotyra), vol. 23, no. 4, pp. 362-371, 2017. https://doi.org/10.5755/j01.ms.23.4.16632
  25. P. Vellaichamy, S. Priyadharshini, and S. Selvan, "Studies on effect of silica fume on workability and strength of concrete," Int. Res. J. Multidiscip. Technovation, vol. 1, no. 6, pp. 165-171, 2019. https://doi.org/10.34256/irjmtcon21
  26. H. M. Hamada, F. Abed, H. Y. B. Katman, A. M. Humada, M. S. Al Jawahery, A. Majdi, S. T. Yousif, and B. S. Thomas, "Effect of silica fume on the properties of sustainable cement concrete," J. Mater. Res. Technol., vol. 24, pp. 8887-8908, 2023. https://doi.org/10.1016/j.jmrt.2023.05.147
  27. M. A. Uddin, M. T. Bashir, A. M. Khan, F. Alsharari, F. Farid, and R. Alrowais, "Effect of silica fume on compressive strength and water absorption of Portland cement-silica fume blended mortar," Arab. J. Sci. Eng., vol. 49, no. 4, pp. 4803-4811, 2024. https://doi.org/10.1007/s13369-023-08204-x
  28. ASTM International, ASTM C109/C109M‑20b: Standard Test Method for Compressive Strength of Hydraulic Cement Mortars, West Conshohocken, PA, USA, 2020.
  29. B. Lothenbach, K. L. Scrivener, and R. D. Hooton, "Supplementary cementitious materials," Cement Concr. Res., vol. 41, no. 3, pp. 217-229, 2011. https://doi.org/10.1016/j.cemconres.2010.12.001
  30. K. Mala, A. K. Mullick, K. K. Jain, et al., "Effect of relative levels of mineral admixtures on strength of concrete with ternary cement blend," Int. J. Concr. Struct. Mater., vol. 7, pp. 239-249, 2013. https://doi.org/10.1007/s40069-013-0049-9
  31. J. Wang, F. Jiang, J. Zhou, and Z. Mao, "The synergistic effect of limestone powder and rice husk ash on the mechanical properties of cement‑based materials," Materials, vol. 17, no. 20, p. 5058, 2024. https://doi.org/10.3390/ma17205058
  32. ASTM International, ASTM C642‑13: Standard Test Method for Density, Absorption, and Voids in Hardened Concrete, West Conshohocken, PA, USA, 2013.
  33. ASTM International, ASTM C597‑16: Standard Test Method for Pulse Velocity Through Concrete, West Conshohocken, PA, USA, 2016.
  34. ASTM International, ASTM C1585‑04 (Reapproved 2013): Standard Test Method for Rate of Absorption of Water by Hydraulic‑Cement Concretes, West Conshohocken, PA, USA, 2013.
  35. L. Breiman, "Random forests," Mach. Learn., vol. 45, no. 1, pp. 5-32, 2001. https://doi.org/10.1023/A:1010933404324