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Search Results for porosity

Article
Comparison of Different Types of Fitness Functions to Choose the Appropriate Attributes for Porosity Prediction

Muna Hadi Saleh, Hadeel M. Tuama

Pages: 737-743

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Abstract

Porosity is one of the most important reservoir characteristics because it indicates to fluid collection. Several techniques used to get good porosity prediction, so, in this study we employed seismic attributes and well log data in a genetic algorithm to get the best porosity prediction. The study attempt to enhance the performance of genetic algorithm for attribute selection and therefore porosity prediction by applying genetic algorithm on different types of fitness functions like average mean square error fitness, average correlation coefficients fitness and performance index fitness. Also, used two methods to represent attributes in genetic algorithm. Different witnesses applied to choose the appropriate fitness function that gives high porosity prediction.

Article
Microstructure and Density Characterization for Nano and Micro Alumina-Aluminum Composites Produced by Powder Metallurgy Process

Abdulrahman Najim Abed, Ban Ali Sabri

Pages: 1024-1033

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Abstract

Al2O3 is a major reinforcement in aluminum-based composites, which have been developing rapidly in recent years. The aim of this paper is to investigate the effect of alumina phases and amounts on the physical properties of fabricated Al-Al2O3 composite. Alpha micro and gamma nano of alumina with particle size of 30µm and 20 nm respectively reinforced aluminum matrix of 45 µm. The percentage of reinforcement material were in the range of (5, 10 and 15wt.%) fabricated by powder metallurgy technique. Specimens dimensions were a disc specimens with 11mm diameter and 5 mm thickness. The green density was achieved under compaction pressure of 500MPa, and then sintered under pressure less sintering at 500ºC in a vacuumed tube furnace for two hours Physical properties of the composite samples have been studied such as relative density, sintered density, porosity, microstructure characteristics, particles distribution, agglomeration, grain sizes and  granularity accumulation distribution. It has been noticed that at the micro alumina phase, its relative densities are decreased when there is an increase in amount of micro alumina addition, on the contrary in case of nano composites, where the relative density are increasing along with the increase in nano alumina addition. At micro and nano composites, the produced relative densities are less than the pure aluminum relative density. Agglomeration are increasing with the increase in amount of reinforcement, while its more obvious with nano composite. Grain size reduced with the increase in amount of alumina in micro and nano composites, while, the obtained average grain size diameter is less in nano composite than in micro composites. It is obvious from the results that the variation in physical properties and microstructure of Al-Al2O3 composite are depends on both of alumina phases (size) and percentages. At 15wt.% of nano alumina higher relative density and lower porosity will be obtained.

Article
The Porosity Effect of Stainless Steel Balls on Forced Convection Pipe Flow

Ayser Munner Flayh, Sajida Lafta Ghashim

Pages: 102-108

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Abstract

An experimental study has been carried out to investigate the effects of stainless-steel balls on forced convection flow in pipe under uniform heat flux. Water is used as the working fluid and stainless-steel balls as a porous media. The Reynolds number range from (5000 to 9000) based on the diameter of the pipe. The experiments were conducted on three various numbers of stainless-steel balls (N) with various diameters (dp), which give various porosity (0.33, 0.38 and 0.41). These are (N= 2400, dp=1mm), (N=1600, dp=3mm) and (N= 750, dp=5mm). Results show that, heat transfer coefficient increases with the decrease in the porosity due to the reduction in the space between balls. This led to an increase in turbulence and produced eddies. Furthermore, enhancement in heat transfer coefficient reached its maximum value of (45%) for ball diameter with (dp=1mm) and water flow rate (9 L/min). New Correlation equations for the average heat transfer coefficient were obtained for three different diameters of balls (1, 3 and 5 mm).

Article
Investigate the Microstructure and the Mechanical Properties of Ni-Ti-Cu Shape Memory Alloys

Dania F. Abbas Aljuboori, Kadhim K. Resan, Ayad M. Takhakh

Pages: 105-112

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Abstract

In this study a Nickel-Titanium-Cupper shape memory alloys was manufactured by powder metallurgy (PM) technique, powder mixture of 50% Ti , 47% Ni and 3% Cu was prepared by mixing for two hours and compacted in a press machine using various compacting pressure (600, 700 and 800) MPa , sample was then sintered for 5 hrs in an electrical tube vacuum furnace using sintering temperature of (850?C, 900?C and 950?C) .phase analysis of samples was conducted by X-ray diffraction test, the effect of different sintering temperature and compacting pressure on the porosity, microhardness ,compression strength and the shape memory effect (SME) was studied, the result showed decrease in the porosity and increasing in the shape recovery ,compression strength and microhardness with increasing compacting pressure and at lower sintering temperature and hence the best results was at 800MPa compacting pressure and 850?C sintering temperature.

Article
Optimization of Nano Hydroxyapatite/chitosan Electrophoretic Deposition on 316L Stainless Steel Using Taguchi Design of Experiments

Mohammed Jasim Kadhim, Nawal Ezzat Abdullatef, Makarim Hazim Abdulkareem

Pages: 1215-1227

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Abstract

The aim of this work is to determine the optimum parameters for deposition of chitosan and mixture of chitosan and hydroxyapatite (HA) layers using electrophoretic deposition.  The layers were on 316L stainless steel substrate. Taguchi approach was utilized to select the optimum parameters for both layers. The parameters used for deposition chitosan are voltage, time and temperature while the parameters used for HA and chitosan are voltage, time, concentration and temperature. Zeta potential tests were employed to measure the solutions stability.  Coating layers were characterized for thickness, porosity and nanoroughness using optical microscopy (OM) and atomic force microscopy (AFM).  The results from Taguchi design of experiments demonstrated that the best conditions for deposition of chitosan and HA layers are  50 V, 5 min, 3 g HA/L and 30°C.    The corresponding thickness, % porosity, nanoroughness and microroughness for optimum conditions were 22 µm, 3.53,  4.48 nm and 3.85 µm respectively.

Article
Porous Silicon Refractive Index Measurements with the Assistance of Two types of Lasers

Saad A. Mohammed Salih

Pages: 1034-1039

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Abstract

Porous Silicon (PSi) samples with (100) orientation n-type were prepared by photo-electrochemical etching process for different variable parameters and fixed electrolyte solution HF:C2H5OH:H2O (2:3:3). Physical and optical properties of PSi would be varied with the variation of process parameters such as current density, anodization time and laser wavelengths. Two types of 50 mW diode lasers were chosen, 473 nm Blue & 532 nm green at 20 mA/cm2 & 15 min etching time to assist the iodization process.  The band gap of the fabricated layer has raised up to (2.9 eV) which is more than twice its original value for the c-Si (1.12 eV). _x000D_ Exploiting the obtained gap energy values, the refractive index of porous silicon layer was calculated depending upon Vandamme empirical relation. It was observed that the porosity is modifiable through etching conditions, which in turn makes refractive index also modifiable. Thus, the calculation depended on taking certain parameters as the current density and etching time in order to compare the effect of applying the two laser wavelengths. AFM was applied to observe the homogeneity and roughness of the PSi mono-layer. The results are in a very good agreement with the range of the refractive indices of PSi and the illumination with green laser gives a better conclusion to use in solar cells as a good absorber and a bad reflector.

Article
Evaluation of Surface Roughness of 316L Stainless Steel Substrate on Nanohydroxyapatite by Electrophoretic Deposition

Mohammed Jasim Kadhim, Nawal Ezzat Abdulateef, Makarim Hazim Abdulkareem

Pages: 28-35

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Abstract

The present work was designed on producing nanohydroxyapatite layers using electrophoretic deposition (EPD) on 316L stainless steel substrate.  The EPD coatings were prepared by the deposition of hydroxyapatite (HA)-chitosan nanocomposites on different substrate roughness (polish surface, 220 grit SiC grind, and sand blast surfaces).  Depositions were performed using the suspensions of HA nano particles (3 g/L) in the mixture of alcohol and distilled water (ethanol, 5 vol. %water and containing 0.5 g/L of chitosan dissolved in 1 vol.% acetic acid.  Coatings were achieved on the cathode at constant voltage, time and temperature (90 V, 5 min and 40 °C respectively); the  pH value was performed and fitted at 4.  After deposition, the coated samples were dried at room temperature for 24 h.  The surface topography of coatings was analyzed using atomic force microscopy (AFM).  SEM was used to postulate both the surface and the cross section morphology of the coatings.  The adhesion bonding between the deposited coatings and substrate were measured using tape tester to evaluate the adhesion bonding between the coating and substrate.  The results showed the deposited coatings on sand blasted substrate has less porosity compared with the polish surface and 220 emery paper SiC grinding substrate respectively.  The coating on the sand blasted substrate showed higher nanoroughness (122 nm), better adhesion bonding (removal area 15%) and higher thickness layer (12 µm) than that of the polish substrate and 220 emery paper SiC grinding substrate.

Article
Improvement Silicon Nanostructured Surface by Laser Induced Etching Process

Marwa Hikmat Ibrahim, Bassam G. Rasheed

Pages: 323-328

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Abstract

Surface reconstruction of silicon using lasers could be utilized to produce silicon nanostructures of various features. Electrochemical and photoelectrochemical etching processes of silicon were employed to synthesize nanostructured surface. Effects of current densities 5, 10 and 20 mA/cm2 on the surface features were examined. It is found that the surface porosity and layer thickness increase with the current density. Moreover, large surface area of 410 m2/cm3 can be achieved when laser power density 0f 0.6 W/cm2 was used during the etching process. Optimum operating conditions were found to achieve better silicon nanostructured surface features. The surface roughness can be reduced to 8.3 nm using laser beam of 650 nm irradiated the silicon surface during the photoelectrochemical etching process. The surface morphology of the nanostructured silicon surface using SEM and AFM could give rich details about the surface. Silver nanoparticles of 10 – 20 nm was embedded at the nanostructured silicon surface by LIFT process to reduce the surface resistance and maintain the large surface area. This technique enables silicon nanostructures to be efficiently used in many optoelectronic applications.

Article
Design and Analysis of Composite Biomaterial Bone Graft Plate

Dunia Abdulsahib Hamdi, Fatima Mowafaq Khider

Pages: 278-285

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Abstract

The mixing technique was applied in this study to enhance the strength performance of the cement. The addition of 3% by weight of hydroxyapatite (HA) nanoparticles were mixed with 97% polymethyl methacrylate (PMMA) acrylic polymer, which has a nano size to serve as the matrix material. The surface roughness and continuous porosity of the bone cement were found to be slightly increased by the incorporation of nanoparticles, which enhanced bone-implant osseointegration and ingrowth. Atomic force microscopy (AFM) analysis revealed that the addition of hydroxyapatite (HAp) nanoparticles resulted in a surface roughness value (Sa) of 16.25 nm, which is similar to that of natural bone. The energy-dispersive X-ray spectroscopy (EDS) mapping results discover precentor material and uniform distribution. The Sample exhibited promising results in the antibacterial test, showing efficacy against bacteria both with and without sterilization, confirming its antibacterial properties. The mechanical tests conducted on the sample, including tensile, compression, bending and Vickers hardness tests, yielded favorable results and indicated that the sample is suitable for its intended application.  In the theoretical works the design of the bone, screw, and bone plate was conducted using SolidWorks, followed by an analysis using ANSYS under both axial and bending load conditions. The theoretical analysis revealed that the safety factor was less than 1 when an axial load of 13 N was applied and a bending load of 2 N was applied, indicating that the structure may not be able to withstand these loads safely. Under both ambient and physiologically relevant conditions in the human body, HA and PMMA have demonstrated to be excellent choices for enhancing the clinical performance of bone cement. This, in turn, can lead to increased longevity of implants, decreased patient risk, and lower healthcare costs

Article
Thermal Performance Enhancement of Phase Change Materials (PCMs) by Using Metal Foams

Ihsan Y. Hussain, Marwah Abdulkareem Jasim

Pages: 235-249

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Abstract

An investigation of thermal conductivity enhancement, melting and solidification processes of Phase Change Materials (PCMs) by using metal foams has been carried out. Two models have been used in the experiments, model I for measuring the effective thermal conductivity of metal foam embedded in paraffin wax, and model II used as a small scale thermal energy storage device with and without metal foam for investigating melting and solidification processes of the PCM under different cooling conditions (natural and forced convection). The theoretical investigation involves analytical solution of two models, the semi-infinite medium for calculating the thermal conductivity, and the thermal energy storage system TESS has been analyzed including several assumptions for determining the convective heat transfer coefficient and the factors that controlling forced convection and solidification of the PCM. The experimental results show that the thermal conductivity of wax with 10 PPI metal foam increased by (37-39) times that of pure wax. Effects of pore density (10 and 40 PPI), metal foam, and mass flow rate on solidification process have been studied and the effects of pore density and metal foam on the melting process have also been investigated. The present experimental results have been compared with the available previous studies and gave a good agreement.

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